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All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Whiskey analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 SPDU
Run date: March 4, 2017
Sample description: Whiskey with DI water
Amount of Sample: 50uL whiskey with 500uL DI water
Sample conditions: 20mL vial with 10 hours equilibration at 25°C and 100RPM
Split Mode: Split for first 2 min, then Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25um film
Column: DB1 30m length x 0.25mm ID, 0.5um film
Carrier: Helium 1.5mL/min
Oven Temp: 35°C hold 5 min, 10°C/min to 150°C, 20°C/min to 300°C, hold 5 min (29 min run time)
GCMS: Agilent 7890B GC 5977A MS
MS Operation: 33-450, 3 scans/sec, 8 min solvent delay

1. 1-Butanol, 3-methyl-, acetate
2. Pentane, 1-(1-ethoxyethoxy)-
3. Hexanoic acid, ethyl ester
4. Butanedioic acid, diethyl ester
5. Octanoic acid, ethyl ester
6. Decanal
7. Fenaclon
8. Nonanoic acid, ethyl ester
9. 2(3H)-Furanone, 5-butyldihydro-4-methyl-, cis
10. Decanoic acid, ethyl ester
11. Dodecanoic acid, ethyl ester

12. Tetradecanoic acid, ethyl ester
13. Isopropyl myristate
14. 2-Pentadecanone, 6,10,14-trimethyl
15. Pentadecanoic acid, ethyl ester
16. 7,9-Di-tert-butyl-1-oxaspiro(4,5)deca-6,9-diene-2,8-dione
17. Ethyl 9-hexadecenoate
18. Hexadecanoic acid, ethyl ester
19. Isopropyl palmitate
20. Oleanitrile
21.Linoleic acid ethyl ester

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