All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Sorbent PenTM Kinetic Study by VASE (Vacuum Assisted Sorbent Extraction) & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: March 21, 2016
Sample description: Geosmin and Halonanisoles spiked into 50mL filtered water
Concentration of Sample: 20ng/L
Sample conditions: 125mL vial + vac + 100rpm agitation + {1,2,3,8,16} hours at 25°C
Split Mode: Splitless
Desorb Conditions: 5min at 260°C
Precolumn: DB1 5m length x 0.25mm ID, 0.5 µm film thickness
Column: DB1 60m length x 0.25mm ID, 0.5 µm film thickness
Carrier: He, 1.5mL/min constant flow
Oven Temp: 35°C, 20°C/min. to 280°C, hold 4min.
GCMS: Agilent 7890B/5977A
MS Operation: 33-350 amu, 2.5 scans/sec

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