All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Raspberry analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: August 2, 2016
Sample description: Fresh Raspberries
Weight of Sample (g): 6.9049
Sample conditions: vac(30sec) + 15hr equilibration
Desorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25µm film
Column: DB1 30m length x 0.25mm ID, 0.5µm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5min., 6°C/min. to 95°C, 10°C/min. to 140°C, 15°C/ min. to 325 hold 5min.
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec

1. 2-Heptanone
2. alpha-pinene
3. beta-myrcene
4. 3-hexen-1-ol, acetate (Z)
5. acetic acid, hexyl ester
6. alpha- phellandrene
7. p-cymene
8. .beta.-Phellandrene
9. gamma terpinene
10. Cyclohexene, 1-methyl-4(1methylethylidene)

11. 3-buten-2-one, 4-(2,6,6 trimethyl 1-cyclohexen-1-yl)
12. 1,1,5-trimethyl-1, 2-hydronaphthalene
13. alpha-lonone
14. 1,3,6,10-Dodecatetraene, 37,11-trimethyl (Z,E)
15. trans-beta-lonone
16. alpha farnesene
17. Naphthalene, 1,2,3,5,6,7,8,8a-octahydro-1,8a-dimethyl-7- (1-methylethenyl)-, [1R-(1.alpha.,7.beta.,8a.alpha.)]-
18. Dodecanoic acid
19.  Pentadecanoic acid
20. n-Hexadecanoic acid

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