All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Mushroom analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: August 22, 2016
Sample description: Mushrooms blended with water (1:2 ratio)Weight of Sample (mL): 7.7366
Weight of Sample (g): 2
Sample Conditions: 40 mL vial with 15 hours equilibration at 25°C
Desorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25µm film
Column: DB1 30m length x 0.25mm ID, 0.5µm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5 min., 10°C/min. to 325C, 325 hold 5 min. (solvent delay at 6 min)
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec

1. Acetic acid
2. 1-Butanol, 3-methyl-
3. Hexanal
4. 1-Hexanol
5. Benzaldehyde
6. 1-Octen-3-one
7. 3-Octanone
8. Octanal
9. Benzeneacetaldehyde
10. 2-Octenal, (E)-

11. 2-Octen-1-ol, (Z)-
12. Propanoic acid, 2-methyl-, 2,2-dimethyl-1- (2-hydroxy-1-methylethyl)propyl ester
13. 5,9-Undecadien-2-one, 6,10-dimethyl-, (E)-
14. Phenol, 2,4-bis(1,1-dimethylethyl)-
15. Benzophenone
16. 1,2-Benzenedicarboxylic acid, bis(2-methylpropyl) ester
17. Dibutyl phthalate
18. Isopropyl palmitate
19. Octadecanoic acid

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