All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM
The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.
Instrument: 5800 HSP
Run date: August 3, 2016
Sample description: Fresh Mango
Weight of sample (g): 7.7366
Sample conditions: 40mL vial with 15 hours equilibration
Dersorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25μm film
Column: DB1 30m length x 0.25mm ID, 0.5μm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: He, 1.5cc/min. constant flow 40°C hold 5min., 6°C/min. to 95°C, 10°C/min. to 140°C, 10°C/ min. to 325 hold 5min.
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec
1. Disulfide, dimethyl
2. Butanoic acid, ethyl ester
3. Butanoic acid, butyl ester
12. Naphthalene, 1,2,3,5,6,7,8,8a-octahydro-1,8a-dimethyl-7-(1-methylethenyl)-, [1R-(1.alpha.,7.beta.,8a.alpha.)]-