All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Gum analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 SPDU Headspace VOC to SVOC
Run date: April 26, 2017
Sample description: Gum
Weight of sample (g): 0.0745
Sample conditions: 20mL vial with 1hour at 25°C 100rpm
Split Mode: Split 2, 30:1
Column: Db-5MS UI 30 x 0.250 x 0.50
Carrier: Helium 1.5mL/min
Oven Temp: 35°C hold 5 min., 10°C/min. to 150, 20°C/min to 300°C, hold 5min (29 min. run time)
GCMS: Agilent 7890B GC 5977A MS
MS Operation: 34-450, 3 scans/sec

1. Propanoic acid, 2-methyl-
2. Butanoic acid, 3-methyl-
3. Butanoic acid, 2-methyl-
4. Heptanal
5. Pyrazine, 2,5-dimethyl-
6. Benzaldehyde
7. Pentanoic acid, 4-methyl-
8. Hexanoic acid
9. Pyrazine, trimethyl-
10. Propanoic acid, 2-hydroxy-, butyl ester
11. D-Limonene
12. Ethanone, 1-(1H-pyrrol-2-yl)-
13. Acetophenone
14. Pyrazine, 3-ethyl-2,5-dimethyl-
15. Pyrazine, tetramethyl-
16. 2-Nonanone
17. Nonanal
18. 1,6-Octadien-3-ol, 3,7-dimethyl-
19. Octanoic acid, ethyl ester
20. Benzeneacetic acid, ethyl ester

21. Acetic acid, 2-phenylethyl ester
22. Benzeneacetaldehyde, .alpha.-ethylidene-
23. Vanillin
24. Benzoic acid, pent-2-yl ester
25. Tetradecane
26. 5-Methyl-2-phenyl-2-hexenal
27. Pentadecane
28. Butylated Hydroxytoluene
29. 1H-2-Benzopyran-1-one, 3,4-dihydro-8-hydroxy-3-methyl-
30. Dodecanoic acid, ethyl ester
31. Benzophenone
32. Tetradecanoic acid, ethyl ester
33. Caffeine
34. 2-Heptadecanone
35. Hexadecanoic acid, methyl ester
36. Di-sec-butyl phthalate
37. 9-Octadecenoic acid, methyl ester
38. Linoleic acid ethyl ester
39. 9-Octadecenoic acid, (E)-
40. Octadecanoic acid, ethyl ester

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