All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Eggnog analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: December 7, 2016
Sample description: Eggnog
Weight of sample (g): 1
Sample conditions: 20mL vial with 2 hours equilibration at 25°C
Desorb Conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25μm film
Column: DB1 30m length x 0.25mm ID, 0.5μm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5 min., 10°C/min. to 300°C, 300°C hold 7 min. (solvent delay at 6 min.)
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec

1. Acetoin
2. Butanoic acid, ethyl ester
3. Furfural
4. 2-Furanmethanol
5. Benzaldehyde
6. D-Limonene
7. Sorbic Acid
8. 2(3H)-Furanone, dihydro-4-hydroxy-
9. Octanoic acid
10. 5-Hydroxymethylfurfural

11. Cinnamaldehyde, (E)-
12. Safrole
13. Eugenol
14. n-Decanoic acid
15. Vanillin
16. Coumarin
17. Tetradecanoic acid
18. n-Hexadecanoic acid
19. cis-Vaccenic acid
20. Octadecanoic acid
21. Glycerol tricaprylate
22. Cholesterol

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