All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Coffee analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: November 28, 2016
Sample description: Breakroom Coffee
Amount of Sample (g): 2
Sample conditions: 20 mL vial with 3 hour equilibration at 60°C
Desorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25µm film
Column: DB1 30m length x 0.25mm ID, 0.5µm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5 min., 10°C/min. to 325C, 325 hold 5 min. (solvent delay at 6 min)
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec
Pen ID: 411-0000008

1. Pyridine
2. 3(2H)-Furanone, dihydro-2-methyl-
3. 3-Furaldehyde
4. 2-Furanmethanol
5. Butyrolactone
6. Ethanone, 1-(2-furanyl)-
7. Pyrazine, 2,5-dimethyl-
8. 2-Furancarboxaldehyde, 5-methyl
9. Phenol
10. 2-Furanmethanol, acetate
11. 1H-Pyrrole-2-carboxaldehyde
12. Ethanone, 1-(1H-pyrrol-2-yl)-
13. Ethanone, 1-(1-methyl-1H-pyrrol-2-yl)-
14. Phenol, 2-methoxy-
15. 1H-Pyrrole, 1-(2-furanylmethyl)-

16. Phenol, 4-ethyl-2-methoxy
17. Indole
18. Furan, 2,2′-[oxybis(methylene)]bis-
19. 2-Methoxy-4-vinylphenol
20. Benzene, 4-ethenyl-1,2-dimethoxy-
21. 1H-Pyrrole, 1-(2-furanylmethyl)-
22. Phenol, 2,5-bis(1,1-dimethylethyl)-
23. Dodecanoic acid, ethyl ester
24. Caffeine
25. 1-Hexadecanol
26. Hexadecanoic acid, methyl ester
27. n-Hexadecanoic acid
28. Isopropyl palmitate
29. Octadecanoic acid
30. Hexadecanamide
31. 9-Octadecenamide, (Z)-

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