All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Cashew analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: November 21, 2016
Sample description: Cashew
Amount of Sample (g): 1
Sample conditions: 40 mL vial with 48 hour equilibration at 25°C
Desorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25µm film
Column: DB1 30m length x 0.25mm ID, 0.5µm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5 min., 10°C/min. to 325C, 325 hold 5 min. (solvent delay at 6 min)
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec
Pen ID: 411-0000004

1. 1H-Pyrrole, 1-methyl
2. Toluene
3. Hexanal
4. Ethylbenzene
5. o-Xylene
6. Bicyclo[4.2.0]octa-1,3,5-triene
7. Pyrazine, 2,5-dimethyl
8. Benzaldehyde
9. Benzeneacetaldehyde
10. D-Limonene
11. Nonanal
12. 4H-Pyran-4-one, 2,3-dihydro-3,5-dihydroxy-6-methyl
13. Dodecane
14. 2-Methoxy-4-vinylphenol
15. 2,4-Decadienal, (E,E)-
16. Tridecane, 5-methyl-

17. Copaene
18. Tetradecane
19. Caryophyllene
20. Humulene
21. Aromandendrene
22. Pentadecane
23. Butylated Hydroxytoluene
24. .beta.-Bisabolene
25. Hexadecane
26. Octadecane
27. Benzene, (1-methylundecyl)-
28. Dibutyl phthalate
29. n-Hexadecanoic acid
30. Isopropyl palmitate
31. 9-Octadecenoic acid, methyl ester, (E)-
32. Diisooctyl phthalate

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