All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent PensTM

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent PensTM combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent PenTM uses an entirely new approach for sample extraction.

Apple analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: August 2, 2016
Sample description: Fresh Gala apple
Weight of Sample (mL): 4.2911
Sample conditions: 15 hours equilibration
Desorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 30m length x 0.25mm ID, 0.5µm film
Column: DB1 30m length x 0.25mm ID, 0.5µm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5min., 6°C/min. to 95°C, 10°C/min. to 140°C, 15°C/min. to 325 hold 5min.
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec

1. Acetic acid, butly ester
2. 1-butanol, 2-methyl acetate
3. acetic acid hexyl ester
4. Limonene
5. Hexanoic acid butyl ester
6. Butanoic acid, 2-methyl-hexyl ester
7. Hexanoic acid hexyl ester
8. alpha-farnescene
9. Octanoic acid-hexyl ester

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