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All studies represented by the chromatogram below have been conducted utilizing Large Volume Static Headspace analysis on the 7650HS-CTS

The all-new 7650HS-CTS is the only commercially available solution that can quantify the consumer experience by taking an equilibrium “snapshot” of the headspace to accurately determine its composition from the lightest through the heaviest compounds. The 7650HS-CTS is truly unique as it is the industries “only” system that uses multiple stages of true capillary columns to perform headspace preconcentration.

Garlic Volatiles Analysis by GC/MS

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Instrument: 7650HS-CTS
Run date: April 20, 2017
Sample description: 1 Clove Chopped Garlic
Weight of sample (g): NA
Sample conditions: 500mL vial with 2 hour equilibration at 25°C
Sample Amount: 100 cc
Split Mode: Splitless
Column: DB1 60m length x 0.32mm ID, 1.0 µm lm
Carrier: He, 2mL/min. constant flow
Oven Temp: 35°C hold 5min., 6°C/min. to 95°C, 10°C/min. to 140°C, 15°C/min. to 230 hold 4.5min.
GCMS: Agilent 7890A/5975C
MS Operation: 33-300 amu, 2.72 scans/sec

1. Hydrogen sulfide
2. Propene
3. Methanethiol
4. Acetaldehyde
5. 1-Propanol
6. Thiirane, methyl
7. Allyl mercaptan
8. Sulfide, allyl methyl
9. Mercaptoacetone
10. Propanoic acid, ethyl ester
11. Disulfide, dimethyl

12. Diallyl sulfide
13. Thiophene, 2,4-dimethyl
14. Disulfide, methyl 2-propeny
15. Disulfide, methyl propyl
16. 1,3-Dithiane
17. Allyl thiopropionate
18. D-Limonene
19. Diallyl disulphide
20. 2-Ethyl[1,3]dithiane
21. Dodecane

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