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All studies represented by the chromatogram below have been conducted utilizing Vacuum Assisted Sorbent Extraction & Headspace Sorbent Pens™

The most versatile extraction and sample preconcentration technology available for GC and GCMS systems. Sorbent Pens™ combine the features of SPME and classical ¼” adsorbent traps in a design with far more flexibility and enhanced performance. The Sorbent Pen™ uses an entirely new approach for sample extraction.

Brie Cheese Duplicate analysis by VASE & Headspace Sorbent Pens

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Instrument: 5800 HSP
Run date: August 15, 2016
Sample description: Brie Cheese
Weight of sample (g): 70g cheese in 140mL water, blended, 10.1025g taken
Sample conditions: blended + vac(30sec) + 50°C + 3 hr equilibration
Desorb conditions: 260°C for 5 min.
Split Mode: Splitless
Precolumn: DB1 5m length x 0.25mm ID, 0.25µm film
Column: DB1 30m length x 0.25mm ID, 0.5µm film
Carrier: He, 1.5cc/min. constant flow
Oven Temp: 40°C hold 5min., 6°C/min. to 95°C, 10°C/min. to 140°C, 10°C/min. to 325 hold 5min.
GCMS: Agilent 7890B/5977A
MS Operation: 34-450 amu, 1.8 scans/sec

1. 4-Heptanone
2. 2-Heptanone
3. Benzaldehyde
4. 2-Octanone
5. Hexanoic acid, ethyl ester
6. Benzeneacetaldehyde
7. 8-Nonen-2-one
8. 2-Nonanone
9. Nonanal
10. Octanoic acid
11. Octanoic acid, ethyl ester
12. Decanal
13. n-Octanoic acid isopropyl ester

14. 2-Undecanone
15. n-Decanoic acid
16. Decanoic acid, ethyl ester
17. 2H-Pyran-2-one, tetrahydro-6-pentyl-
18. 2-Tridecanone
19. Dodecanoic acid
20. Dodecanoic acid, ethyl ester
21. 2H-Pyran-2-one, 6-heptyltetrahydro-
22. Tetradecanoic acid
23. n-Hexadecanoic acid
24. Hexadecanoic acid, ethyl ester

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